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4 recordsLinked to original sources
USGS2001

Standard Reference Material (SRM 1990) for Single Crystal Diffractometer Alignment

An international project was successfully completed which involved two major undertakings: (1) a round-robin to demonstrate the viability of the selected standard and (2) the certification of the lattice parameters of the SRM 1990, a Standard Reference Material?? for single crystal diffractometer alignment. This SRM is a set of ???3500 units of Cr-doped Al2O3, or ruby spheres [(0 420.011 mole fraction % Cr (expanded uncertainty)]. The round-robin consisted of determination of lattice parameters of a pair of crystals' the ruby sphere as a standard, and a zeolite reference to serve as an unknown. Fifty pairs of crystals were dispatched from Hauptman-Woodward Medical Research Institute to volunteers in x-ray laboratories world-wide. A total of 45 sets of data was received from 32 laboratories. The mean unit cell parameters of the ruby spheres was found to be a=4.7608 A?? ?? 0.0062 A??, and c=12.9979 A?? ?? 0.020 A?? (95 % intervals of the laboratory means). The source of errors of outlier data was identified. The SRM project involved the certification of lattice parameters using four well-aligned single crystal diffractometers at (Bell Laboratories) Lucent Technologies and at NRC of Canada (39 ruby spheres), the quantification of the Cr content using a combined microprobe and SEM/EDS technique, and the evaluation of the mosaicity of the ruby spheres using a double-crystal spectrometry method. A confirmation of the lattice parameters was also conducted using a Guinier-Ha??gg camera. Systematic corrections of thermal expansion and refraction corrections were applied. These rubies_ are rhombohedral, with space group R3c. The certified mean unit cell parameters are a=4.76080 ?? 0.00029 A??, and c=12 99568 A?? ?? 0.00087 A?? (expanded uncertainty). These certified lattice parameters fall well within the results of those obtained from the international round-robin study. The Guinier-Ha??gg transmission measurements on five samples of powdered rubies (a=4.7610 A?? ?? 0.0013 A??, and c=12.9954 A?? ?? 0.0034 A??) agreed well with the values obtained from the single crystal spheres.

Journal of Research of the National Institute of S↗
USGS2007

Antarctica: A Keystone in a Changing World--Online Proceedings for the Tenth International Symposium on Antarctic Earth Sciences. Santa Barbara, California, U.S.A.--August 26 to September 1, 2007

Overview: The International Symposium on Antarctic Earth Sciences (ISAES) is held once every four years to provide an international forum for presenting research results and new ideas and for planning future Antarctic geoscience research projects. This Tenth ISAES coincides with the International Polar Year (IPY; 50th Anniversary of the International Geophysical Year) and has been structured to showcase the great breadth of geoscience research being done in Antarctic regions by more than more than 100 institutions located in over 30 countries. The science program of the Symposium encompasses six broad themes that cover key topics on evolution and interactions of the geosphere, cryosphere and biosphere and their cross-linkages with past and historic paleoclimates. Emphasis is also on deciphering the climate records in ice cores, geologic cores, rock outcrops and those inferred from climate models. New technologies for the coming decades of geoscience data collection are also highlighted. Ten keynote presentations at the symposium outline the foundation for the research sessions of the symposium and the structure of the Online Proceedings and Proceedings Book for the Tenth ISAES. The ISAES is traditionally a cornerstone meeting for the Scientific Committee on Antarctic Research (SCAR). In recognition of the Tenth ISAES being held in the U.S. for the first time in 30 years and during IPY, the publication of the symposium proceedings is being handled as a special collaborative effort of the U.S. National Science Foundation, the U.S. Geological Survey, The National Academies Polar Research Board and The National Academies Press. The National Academies Polar Research Board oversees the activities of SCAR in the U.S. Special attention has been directed at publication formats for the symposium, to expedite the open and wide sharing of mature and preliminary research results presented in talks and posters at the Tenth ISAES. All symposium presentations are documented by a short Summary printed in the Symposium Program Booklet and either a short research paper or an extended abstract. The research papers and extended abstracts are compiled in this Online Proceedings and are replicated on a DVD-ROM that is placed in the back of the Tenth ISAES Proceedings Book. The Proceedings Book has printed versions of the keynote talks and an overview paper of the symposium. The short research papers and extended abstracts have been handled differently. Research papers present mature research results and syntheses. They have been peer-reviewed using standard journal procedures. Following revisions and acceptances by co-editors, the papers have been formatted for publication and proofread by authors. Each paper has been assigned a Digital Object Identification (DOI) number and separate html link, and posted online (as part of this USGS Open-File Report series) to ensure open and wide access to the research results. Extended abstracts focus on preliminary research results and have not been peer reviewed. They have had only minimal editorial review and revision. Authors have formatted and proofread their papers. Extended abstracts were not given DOI numbers and are included together in a separate chapter of this online Proceedings. USGS publications staff and Stanford-student editorial assistants indexed and compiled the PDF versions of the short research papers and extended abstracts for inclusion in this online Proceedings. USGS staff created the master DVD-ROM that contains a replica of the Online Proceedings for the Tenth ISAES, and provided the DVD-ROM copies that are included in the Tenth ISAES Proceedings Book published by The National Academies Press in the U.S. A team of more than 25 co-editors coordinated with the numerous authors and peer reviewers in handling the many research papers and extended abstracts that are included herein. Handling the large volume of short papers and extended abstracts, getting most of them onli

Open-File Report↗
USGS2003

Seabird tissue archival and monitoring project: Egg collections and analytical results 1999-2002

In 1998, the U.S. Geological Survey Biological Resources Division (USGS-BRD), the U.S. Fish and Wildlife Service (USFWS) Alaska Maritime National Wildlife Refuge (AMNWR), and the National Institute of Standards and Technology (NIST) began the Seabird Tissue Archival and Monitoring Project (STAMP) to collect and cryogenically bank tissues from seabirds in Alaska for future retrospective analysis of anthropogenic contaminants. The approach of STAMP was similar to that of the Alaska Marine Mammal Tissue Archival Project (AMMTAP). AMMTAP was started in 1987 by NIST and the National Oceanic and Atmospheric Administration (NOAA) as part of the Outer Continental Shelf Environmental Assessment Program sponsored by the Minerals Management Service. Presently sponsored by the USGS-BRD, AMMTAP continues its work as part of a larger national program, the Marine Mammal Health and Stranding Response Program. AMMTAP developed carefully designed sampling and specimen banking protocols. Since 1987, AMMTAP has collected tissues from marine mammals taken in Alaska Native subsistence hunts and has cryogenically banked these tissues at the NIST National Biomonitoring Specimen Bank (NBSB). Through its own analytical work and working in partnership with other researchers both within and outside Alaska, AMMTAP has helped to develop a substantial database on contaminants in Alaska marine mammals. In contrast, data and information is limited on contaminants in Alaska seabirds, which are similar to marine mammals in that they feed near the top of the food chain and have the potential for accumulating anthropogenic contaminants. During its early planning stages, STAMP managers identified the seabird egg as the first tissue of choice for study by the project. There is a relatively long history of using bird eggs for environmental monitoring and for investigating the health status of bird populations. Since 1998, protocols for collecting and processing eggs, and cryogenically banking egg samples have been developed by STAMP (see York et al. 2001). Eggs are being collected on an annual basis for several species at nesting colonies throughout Alaska. Aliquots of these egg samples are being analyzed on a regular basis for persistent organic pollutants and mercury. Results of this work have been published in scientific journals (Christopher et al. 2002) and in conference proceedings (Kucklick et al. 2002; Vander Pol et al. 2002a, 2002b). The intent of this report is to provide an up-to-date description of STAMP. The report contains the most recent egg collection inventory, analytical data, preliminary interpretations based on these data, and a discussion of possible future directions of the project.

Report↗
USGS2002

U.S. Geological Survey spatial data access

The U.S. Geological Survey (USGS) has done a progress review on improving access to its spatial data holdings over the Web. The USGS EROS Data Center has created three major Web-based interfaces to deliver spatial data to the general public; they are Earth Explorer, the Seamless Data Distribution System (SDDS), and the USGS Web Mapping Portal. Lessons were learned in developing these systems, and various resources were needed for their implementation. The USGS serves as a fact-finding agency in the U.S. Government that collects, monitors, analyzes, and provides scientific information about natural resource conditions and issues. To carry out its mission, the USGS has created and managed spatial data since its inception. Originally relying on paper maps, the USGS now uses advanced technology to produce digital representations of the Earth’s features. The spatial products of the USGS include both source and derivative data. Derivative datasets include Digital Orthophoto Quadrangles (DOQ), Digital Elevation Models, Digital Line Graphs, land-cover Digital Raster Graphics, and the seamless National Elevation Dataset. These products, created with automated processes, use aerial photographs, satellite images, or other cartographic information such as scanned paper maps as source data. With Earth Explorer, users can search multiple inventories through metadata queries and can browse satellite and DOQ imagery. They can place orders and make payment through secure credit card transactions. Some USGS spatial data can be accessed with SDDS. The SDDS uses an ArcIMS map service interface to identify the user’s areas of interest and determine the output format; it allows the user to either download the actual spatial data directly for small areas or place orders for larger areas to be delivered on media. The USGS Web Mapping Portal provides views of national and international datasets through an ArcIMS map service interface. In addition, the map portal posts news about new map services available from the USGS, many simultaneously published on the Environmental Systems Research Institute Geography Network. These three information systems use new software tools and expanded hardware to meet the requirements of the users. The systems are designed to handle the required workload and are relatively easy to enhance and maintain. The software tools give users a high level of functionality and help the system conform to industry standards. The hardware and software architecture is designed to handle the large amounts of spatial data and Internet traffic required by the information systems. Last, customer support was needed to answer questions, monitor e-mail, and report customer problems.

Journal of Geospatial Engineering↗