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At least 163 records · Page 9Linked to original sources

USGS2006

Analysis of trace metals in water by inductively coupled plasma emission spectrometry using sodium dibenzyldithiocarbamate for preconcentration

Since concentrations of trace elements in most natural waters seldom exceed the μg/L level, analysis of trace elements in natural waters by inductively coupled plasma emission spectrometry (ICP) requires a preconcentration procedure. The elements Ag, Bi, Cd, Co, Cu, Fe, Mo, Ni, Pb, Sn, V, W, and Zn were separated and concentrated from 500 mL of water by coprecipitating them with sodium dibenzyldithiocarbamate (NaDBDTC) using nickel or silver as a carrier. The precipitated trace elements were collected on a membrance filter, redissolved from the filter with hot nitric and hydrochloric acids, and analyzed using ICP. Recoveries for all the trace elements except tungsten exceeded 80%. Coprecipitation of trace elements with NaDBDTC eliminated the use of difficult-to-inject organic solvents, and NaDBDTC coprecipitated a wider array of trace elements than ammoniumpyrrolidinedithiocarbamate (APDC), another commonly used coprecipitate.

Analytical Letters↗

USGS1998

The use of synthesized aqueous solutions for determining strontium sorption isotherms

The use of synthesized aqueous solutions for determining experimentally derived strontium sorption isotherms of sediment was investigated as part of a study accessing strontium chemical transport properties. Batch experimental techniques were used to determine strontium sorption isotherms using synthesized aqueous solutions designed to chemically represent water from a natural aquifer with respect to major ionic character and pH. A strontium sorption isotherm for a sediment derived using a synthesized aqueous solution was found to be most comparable to an isotherm derived using natural water when the synthesized aqueous solution contained similar concentrations of calcium and magnesium. However, it is difficult to match compositions exactly due to the effects of disequilibrium between the solution and the sediment. Strong linear relations between sorbed strontium and solution concentrations of calcium and magnesium confirm that these cations are important co-constituents in these synthesized aqueous solutions. Conversely, weak linear relations between sorbed strontium and solution concentrations of sodium and potassium indicate that these constituents do not affect sorption of strontium. The addition of silica to the synthesized aqueous solution does not appreciably affect the resulting strontium sorption isotherm.

Journal of Contaminant Hydrology↗

USGS1970

Temperature and water-quality conditions of the Patuxent River estuary, Maryland, January 1966 through December 1967

The effect of power plant cooling water in raising natural water temperatures at a location near the power plant on the Patuxent River estuary is clearly evident from thermograph records. Surface temperature at a station 333 m (1,000 ft) downstream from the discharge canal was raised an average of about 4 C, and at times by as much as 8 C. Temperature rises were greatest during the winter. Infrared imagery showed that elevated surface temperatures could be detected about 5.5 km (3 nautical miles) upstream at flood tide. Temperature profiles obtained from airborne radiation equipment revealed a complicated surface temperature pattern and also showed the effects of density differences and wind action on the steam-electric station (S.E.S.) effluent plume. Mean annual salinity for a 5-year period (1963–1967) was highest in 1966, about 12.3 ‰, and lowest in 1967, about 9.9‰. Dissolved oxygen values for 1966–1967 ranged from 3.2 to 15.6 mg/l, and saturation ranged from 55 to 152%. Turbidity levels were inversely related to salinity, with the highest annual, mean of 28 JCU (Jackson Candle Units) occurring in 1967, the lowest salinity year. The extreme tide range was 2.1 m (6.7 ft); mean water levels at the Patuxent Bridge were highest in summer and lowest in winter. Water stages are more affected by wind speed and direction than by flow in the river.

Maryl↗

USGS2013

Economic resilience through "One-Water" management

Disruption of water availability leads to food scarcity and loss of economic opportunity. Development of effective water-resource policies and management strategies could provide resiliance to local economies in the face of water disruptions such as drought, flood, and climate change. To accomplish this, a detailed understanding of human water use and natural water resource availability is needed. A hydrologic model is a computer software system that simulates the movement and use of water in a geographic area. It takes into account all components of the water cycle--“One Water”--and helps estimate water budgets for groundwater, surface water, and landscape features. The U.S. Geological Survey MODFLOW One-Water Integrated Hydrologic Model (MODFLOWOWHM) software and scientific methods can provide water managers and political leaders with hydrologic information they need to help ensure water security and economic resilience.

Open-File Report↗

USGS2026

Informing policy response to declining water supply in the Colorado River basin: Linking water supply management with outcomes for fish communities

Water-supply managers in the Colorado River Basin are tasked with balancing consumptive water use with natural water supply. Decisions associated with water-supply policy can include where and how much water consumption occurs, where water could be stored, and how to operate reservoirs. Water-supply decisions often affect other resources including energy production, recreation and aquatic ecosystems. The goal of this project was to model how different water supply management scenarios might affect riverine ecosystems with a specific focus on potential impacts on federally listed fish populations, including threatened humpback chub (Gila cypha) and endangered Colorado pikeminnow (Ptychocheilus lucius) and razorback sucker (Xyrauchen texanus). Threats to these endemic species include introduced non-native fish species that often become invasive, like smallmouth bass (Micropterus dolomieu), and altered physical conditions that may favor these non-native fish species over the endemic fish species. Changes in how water supply may be managed in the Colorado River Basin can affect physical conditions in rivers by altering how much water flows through a particular river segment at a given time, by changing the extent of riverine ecosystems between reservoirs, and by determining the quality of water released from storage reservoirs with fixed release elevation (e.g., full reservoirs generally release colder water). To address our goal, we developed tools that coupled water storage models, river temperature models and fish population models to examine how different scenarios to operate Lake Mead, Lake Powell, and Flaming Gorge Reservoir, the three largest reservoirs in the watershed, may affect fish populations. We developed our work plan when available water supply was diminished. At the end of our project period (May 2022), Lake Powell and Lake Mead contained historically low water levels, and our models were being used in evaluating different options for operating Lake Powell by the Bureau of Reclamation and other stakeholders.

Arizona, Utah, Wyoming↗

USGS2025

Preserving and increasing water resources—Natural infrastructure in dryland streams in Baja California Sur, Mexico

The Los Planes watershed of Baja California Sur, Mexico, and its underlying aquifer are experiencing groundwater decline owing to low average annual rainfall (28.1 centimeters per year) and rising water demand from population growth and agricultural activities. This decline in water availability can lead to desertification—a process that changes arable land to desert by degrading soil and vegetation—and can pose serious challenges to livelihoods that depend on the land. To address these issues, a ranch in the Los Planes watershed has installed many natural infrastructures in dryland streams (NIDS) in channels for soil and water conservation. In 2022, the U.S. Geological Survey (USGS) began working with regional researchers and land managers to investigate the effects of NIDS on natural biological, geochemical, and physical processes and determine the efficacy of NIDS for water augmentation in the Los Planes watershed. The USGS also worked with local academic institutions and nonprofit organizations to create public educational opportunities focused on the area’s hydrogeology. These and other collaborative efforts with the U.S. Water Partnership and Innovaciones Alumbra aim at enhancing water resources in the Baja California Sur region and promoting water security and safeguarding community well-being. Resume La cuenca de Los Planes, ubicada en Baja California Sur, México, y su acuífero subyacente, están sufriendo una disminución de las aguas subterráneas debido a la baja precipitación media anual (28.1 centímetros por año) y la alta demanda de agua por parte de una población creciente y la actividad agrícola. Esta disminución de la disponibilidad de agua puede conducir a la desertificación—un proceso que por medio de la degradación del suelo y la vegetación convierte a la tierra cultivable en desierto—representando un serio desafío para los medios de vida de las personas. Para abordar estos problemas, un rancho en la cuenca de Los Planes ha instalado numerosas obras de Infraestructura Natural en Arroyos de Tierras Áridas (INATS) para conservación del suelo y del agua. En 2022, el Servicio Geológico de los Estados Unidos (USGS, por sus siglas en inglés) comenzó a trabajar con investigadores regionales y gestores de tierras para estudiar los efectos de INATS en los procesos biológicos, geoquímicos y físicos, y determinar su eficacia en el aumento de los recursos hídricos en la cuenca de Los Planes. El USGS se ha asociado con instituciones académicas y organizaciones locales sin fines de lucro para crear oportunidades educativas públicas centradas en la hidrogeología de la zona. Estos y otros esfuerzos colaborativos con la Asociación del Agua de Estados Unidos (U.S. Water Partnership) e Innovaciones Alumbra, tienen como objetivo mejorar el uso de los recursos hídricos en la región de Baja California Sur, promover la seguridad hídrica y proteger el bienestar de la comunidad.

Baja California Sur↗

USGS1975

Water-quality data from oil and gas wells in part of the Permian Basin, southeastern New Mexico and western Texas

Approximately 8,000 chemical analyses of water produced from formations of several geologic ages in south eastern New Mexico and western Texas are tabulated by both geographic location and geologic formation. Empirical and mathematical relationships between (1) the dissolved solids and the measured and computed resistivity of water, the chloride-ion concentration and the density, and (2) the concentration of chloride-ion and the density and the resistivity of water, were established. Resistivities of water computed following a method developed by Moore, Szasz, and Whitney (1966) using the concentration of the six most common constituents dissolved in natural water correlate favorably with the measured resistivities of natural water. The water analyses were obtained chiefly from oil companies and oil-service companies operating in the western part of the Permian basin. The data were associated with the proper well by searching location, operator, and reference number cross indexes prepared from the Permian Basin Well Data System files. The cross indexes were determined to be essential to efficient data processing operations. After preliminary screening for nonrepresentative data, all data were indexed to the Permian Basin Well Data System magnetic tape file scout records by the unique reference number. The data were then coded, punched into tabulating cards, and stored on magnetic tape for computer operations. Data verification steps not normally required when using data received from a laboratory following standardized analytical techniques on samples obtained under standardized and controlled procedures were performed in order to upgrade reliability of the information. Data errors detected included poorly located or identified samples; mistakes including reproducing, or key punching; laboratory errors; inconsistent reporting; and nonrepresentative or contaminated samples.

New Mexico, Texas↗

USGS1984

The concept of electron activity and its relation to redox potentials in aqueous geochemical systems

The definition of a formal thermodynamic activity of electrons in redox reactions appears in the literature of the 1920's. The concept of pe as -log (electron activity) was introduced by Jorgensen in 1945 and popularized in the geochemical literature by Sillen, who considered pe and pH as master variables in geochemical reactions. The physical significance of the concept of electron activity was challenged as early as 1928. However, only in the last two decades have sufficient thermodynamic data become available to examine this question quantitatively. The chemical nature of hydrated electrons differs greatly from that of hydrated protons, and thermodynamic data show that hydrated electrons cannot exist at physically meaningful equilibrium concentrations under natural conditions. This has important consequences for the understanding of redox processes in natural waters. These are: (1) the analogy between pe and pH as master variables is generally carried much further than is justified; (2) a thermodynamically meaningful value of redox potential cannot be assigned to disequilibrium systems; (3) the most useful approach to the study of redox characteristics is the analysis and study of multiple redox couples in the system; and (4) for all practical purposes, thermodynamically defined redox potentials do not exist (and thus cannot be measured) in natural waters. The overall implication for natural systems is that, in terms of redox reactions, each case must be considered on an individual and detailed basis. Field studies would appear to be a mandatory part of any site-specific study; conclusions regarding redox processes cannot be based solely on electrode measurements or thermodynamic stability calculations. (USGS)

Open-File Report↗

USGS2021

Chapter A6.4. Measurement of pH

The “National Field Manual for the Collection of Water-Quality Data” (NFM) provides guidelines and procedures for U.S. Geological Survey (USGS) personnel who collect data used to assess the quality of the Nation’s surface-water and groundwater resources. This chapter, NFM A6.4, provides guidance and protocols for the measurement of pH of a water sample, which include the scientific basis of the measurement, selection and maintenance of equipment, calibration, procedures for measurement and reporting, and troubleshooting. It updates and supersedes USGS Techniques of Water-Resources Investigations, book 9, chapter A6.4, version 2.0, by G.F. Ritz and J.A. Collins. The pH of natural waters is routinely measured when water samples are collected, is often measured continually at USGS streamgages, and is a parameter regularly measured during laboratory and field experiments. The field methods for measuring pH described in this chapter are applicable to most natural waters. Before 2017, the NFM chapters were released in the USGS Techniques of Water-Resources Investigations series. Effective in 2018, new and revised NFM chapters are being released in the USGS Techniques and Methods series; this series change does not affect the content and format of the NFM. More information is in the general introduction to the NFM (USGS Techniques and Methods, book 9, chapter A0) at https://doi.org/10.3133/tm9A0 . The authoritative current versions of NFM chapters are available in the USGS Publications Warehouse at https://pubs.er.usgs.gov/ . Comments, questions, and suggestions related to the NFM can be addressed to nfm@usgs.gov .

Techniques and Methods↗

USGS1971

An evaluation of procedures used in computing chemical denudation rates

Computations of chemical denudation rates (that is, the average rate of lowering of the earth's crust by chemical processes) should be based only upon those components of dissolved loads of streams that are derived from chemical weathering of rocks and soils, even though identification of those components is difficult and imprecise. Past computations of chemical denudation rates exaggerated by 1.4 to 2.4 times the significance of this process because they were calculated from total dissolved loads. Identification of separate denudation and nondenudation components in a water analysis can be done most readily for streams in crystalline silicate rock terrane where commonly 25 to 55 percent of the dissolved solids are HCO 3 −1 , SO 4 −2 , Cl −1 , and NO 3 −1 that cannot be derived from the underlying rock; instead these ions are derived either directly from the atmosphere or from atmosphere-biosphere interactions. Most of the remaining solutes are derived from chemical weathering or rainfall, or both. Existing data are often insufficient to separate these two components, but atmospheric contributions to dissolved loads of dilute natural waters are substantial. The commonly observed increased concentration of dissolved solids in chemically polluted rivers is produced by concentration of natural dissolved loads by evaporation, and by addition of solutes not present in natural waters. Concentration of natural solutes represents a modification of natural denudation processes that does not change the rate of denudation. Addition of new solutes represents man-induced, accelerated chemical denudation. Extrapolation of modern chemical denudation rates to geologic situations is extremely imprecise because of uncertainties in assessing man's influence on present dissolved loads, in reconstructing the number and magnitude of past climatic changes, and in evaluating the effects of evolving flora and fauna.

Bulletin of the Geological Society of America↗

USGS1986

Determination of Ca, Mg, Na, Cd, Cu, Fe, K, Li and Zn in acid mine and reference water samples by inductively coupled plasma atomic fluorescence spectrometry

An inductively coupled plasma atomic fluorescence spectrometric (ICP-AFS) method was used for the determination of nine elements in natural water. Reference and acid mine water samples were analysed by this method to demonstrate its usefulness for hydrogeochemical exploration. The elements were determined in two groups based on the compatibility of operating conditions and consideration of element abundance levels in natural water. Ca, Mg and Na were determined as a group using one set of instrumental conditions and a 1 + 99 dilution of the sample, and Cd, Cu, Fe, K, Li and Zn were determined using another set of conditions and the undiluted sample. The detection limits for the elements are as follows: Ca, 1.4; Mg, 1.7; Na, 2.0; Cd, 1.8; Cu, 6.2; Fe, 15.8; K, 3.5; Li, 0.3; and Zn, 1.2 ng ml –1 . Each element has a linear range spanning about four orders of magnitude. The method has good precision and accuracy, as shown by statistics on replicate analyses and by the agreement between values obtained and those recommended for the reference water samples, and also those obtained by atomic absorption spectrometry for the acid mine water samples.

The Analyst↗

USGS2009

Integrated treatment process using a natural Wyoming clinoptilolite for remediating produced waters from coalbed natural gas operations

Coalbed natural gas (CBNG) development in western U.S. states has resulted in an increase in an essential energy resource, but has also resulted in environmental impacts and additional regulatory needs. A concern associated with CBNG development relates to the production of the copious quantities of potentially saline-sodic groundwater required to recover the natural gas, hereafter referred to as CBNG water. Management of CBNG water is a major environmental challenge because of its quantity and quality. In this study, a locally available Na-rich natural zeolite (clinoptilolite) from Wyoming (WY) was examined for its potential to treat CBNG water to remove Na+ and lower the sodium adsorption ratio (SAR, mmol1/2 L- 1/2). The zeolite material was Ca-modified before being used in column experiments. Column breakthrough studies indicated that a metric tonne (1000??kg) of Ca-WY-zeolite could be used to treat 60,000??L of CBNG water in order to lower SAR of the CBNG water from 30 to an acceptable level of 10??mmol1/2 L- 1/2. An integrated treatment process using Na-WY-zeolite for alternately treating hard water and CBNG water was also examined for its potential to treat problematic waters in the region. Based on the results of this study, use of WY-zeolite appears to be a cost-effective water treatment technology for maximizing the beneficial use of poor-quality CBNG water. Ongoing studies are evaluating water treatment techniques involving infiltration ponds lined with zeolite. ?? 2008 Elsevier B.V. All rights reserved.

Applied Clay Science↗

USGS2012

Geochemistry of water

The quadrennium 1967–1970 has been a productive period in the field of water geochemistry. Field studies, laboratory investigations, and theoretical considerations have led to significant advances in our knowledge of the chemical behavior of natural waters and of the solid earth materials that contain them. A symposium on trace inorganics in water, sponsored by the American Chemical Society, was held in Miami, Florida, in 1967. The proceedings of this conference were published in 1968 in the Advances in Chemistry Series 73. This volume deals with the occurrence, behavior, and analysis of inorganic constituents in natural waters.

Eos, Transactions, American Geophysical Union↗

USGS2004

The case for regime-based water quality standards

Conventional water quality standards have been successful in reducing the concentration of toxic substances in US waters. However, conventional standards are based on simple thresholds and are therefore poorly structured to address human-caused imbalances in dynamic, natural water quality parameters, such as nutrients, sediment, and temperature. A more applicable type of water quality standarda??a a??regime standarda??a??would describe desirable distributions of conditions over space and time within a stream network. By mandating the protection and restoration of the aquatic ecosystem dynamics that are required to support beneficial uses in streams, well-designed regime standards would facilitate more effective strategies for management of natural water quality parameters.

BioScience↗

USGS1974

Determination of selenium in water

The determination of selenium by hydride generation atomic absorption spectrophotometry using zinc is widely used. Very little is mentioned, however, on possible interferences. In an attempt to use this technique for the determination of selenium in natural waters, interferences were found. The most serious interference occurred when arsenic was present. As little as 5 μg of arsenic/l suppressed the formation of selenium hydride. Because arsenic may be present with selenium in natural waters, the above method was abandoned in favor of the following atomic absorption spectrophotometric method for the determination of both inorganic and organically bound selenium. Organic selenium compounds, if present, are first decomposed by digestion with potassium permanganate in hot acid solution. The solution is then made basic and the solution evaporated to dryness in the presence of calcium chloride which prevents the loss of selenate during the evaporation. Hydrochloric acid is added to the residue to reduce the selenate to selenite. Quantitative reduction is obtained without loss of selenium by controlling the temperature, time, and acid concentration. It should be emphasized that the selenium must be in the selenite form prior to its final reduction. The selenium is finally liberated from 6M hydrochloric acid solution with stannous chloride and the selenium hydride vapor subsequently removed from solution by aeration and swept by a flow of nitrogen into a hydrogen flame where it is determined by atomic absorption at 196.0 nm. The method may be used to analyze water samples containing at least 2 μg/l of selenium.

Atomic Absorption Newsletter↗

USGS2025

The effects of breeding status on common raven movement, home range, and habitat selection

Anthropogenic infrastructure has contributed to increasing common raven ( Corvus corax ) abundance across the Great Basin region of the United States, particularly in sagebrush ecosystems, where high raven densities are correlated with reduced sage-grouse ( Centrocercus urophasianus ) nest survival. Our understanding of how raven reproductive behavior affects sage-grouse nest predation is limited, especially considering their overlapping breeding seasons. Understanding differences in space use and resource selection between breeding and non-breeding ravens could help identify high-use areas and corresponding predation risk for sage-grouse nests. We analyzed space use and resource selection of breeding ( n = 13) and non-breeding ( n = 32) global positioning system (GPS)-marked ravens in Nevada, USA (2017–2022) during the breeding season (1 March–31 June). We compared home-range size, core area size, step lengths, and resource selection within a Bayesian framework with inference made by comparing Bayesian credible intervals (CRI). We generated home range and core area estimates using autocorrelated kernel density methods. We did not find a difference in home range size between breeding (469.33 km 2 , 95% CRI = 228.79–709.45 km 2 ) and non-breeding (525.26 km 2 , 95% CRI = 410.71–654.10 km 2 ) ravens. However, breeding ravens had smaller core areas (10.77 km 2 , 95% CRI = 3.16–35.78 km 2 ) and shorter step lengths (1,160.33 m/hr, 95% CRI = 1,087.78–1,277.17 m/hr) than non-breeding ravens (core area = 279.50 km 2 , 95% CRI = 206.77–363.72 km 2 ; step length = 1,953.74 m/hr, 95% CRI = 1,898.42–2,009.56 m/hr). Ravens in both breeding classes selected high normalized difference vegetation index (NDVI) and low annual grass and shrub cover, but non-breeding ravens showed stronger selection for low annual grass and shrub cover areas. We found strong differences in selection between breeding classes for 6 of our 9 covariates: distance to road, solar radiation, distance to natural water, distance to forest edge, percent annual grass cover, and percent shrub cover. Non-breeding ravens concentrated activity near forest edges, natural water sources, and anthropogenic features, whereas breeding ravens focused activity close to their nests. Our findings suggest that raven management could be more effective if it targeted areas with high NDVI and low annual grass and shrub cover, especially in anthropogenically modified landscapes and near forest edges, and prevented raven nest establishment near prey populations of concern.

Nevada↗

USGS2002

Corn leaf nitrate reductase - A nontoxic alternative to cadmium for photometric nitrate determinations in water samples by air-segmented continuous-flow analysis

Development, characterization, and operational details of an enzymatic, air-segmented continuous-flow analytical method for colorimetric determination of nitrate + nitrite in natural-water samples is described. This method is similar to U.S. Environmental Protection Agency method 353.2 and U.S. Geological Survey method 1-2545-90 except that nitrate is reduced to nitrite by soluble nitrate reductase (NaR, EC 1.6.6.1) purified from corn leaves rather than a packed-bed cadmium reactor. A three-channel, air-segmented continuous-flow analyzer-configured for simultaneous determination of nitrite (0.020-1.000 mg-N/L) and nitrate + nitrite (0.05-5.00 mg-N/L) by the nitrate reductase and cadmium reduction methods-was used to characterize analytical performance of the enzymatic reduction method. At a sampling rate of 90 h-1, sample interaction was less than 1% for all three methods. Method detection limits were 0.001 mg of NO2- -N/L for nitrite, 0.003 mg of NO3-+ NO2- -N/L for nitrate + nitrite by the cadmium-reduction method, and 0.006 mg of NO3- + NO2- -N/L for nitrate + nitrite by the enzymatic-reduction method. Reduction of nitrate to nitrite by both methods was greater than 95% complete over the entire calibration range. The difference between the means of nitrate + nitrite concentrations in 124 natural-water samples determined simultaneously by the two methods was not significantly different from zero at the p = 0.05 level.

Environmental Science & Technology↗

USGS1985

Chemistry and transport of soluble humic substances in forested watersheds of the Adirondack Park, New York

Studies were conducted in conjunction with the Integrated Lake-Watershed Acidification Study (ILWAS) to examine the chemistry and leaching patterns of soluble humic substances in forested watersheds of the Adirondack region. During the summer growing season, mean dissolved organic carbon (DOC) concentrations in the ILWAS watersheds ranged from 21–32 mg C l −1 in O/A horizon leachates, from 5–7 mg C l −1 in B horizon leachates, from 2–4 mg C l −1 in groundwater solutions, from 6–8 mg C l −1 in first order streams, from 3–8 mg C l −1 in lake inlets, and from 2–7 mg C l −1 in lake outlets. During the winter, mean DOC concentrations dropped significantly in the upper soil profile. Soil solutions from mixed and coniferous stands contained as much as twice the DOC concentration of lysimeter samples from hardwood stands. Results of DOC fractionation analysis showed that hydrophobia and hydrophilic acids dominate the organic solute composition of natural waters in these watersheds. Charge balance and titration results indicated that the general acid-base characteristics of the dissolved humic mixture in these natural waters can be accounted for by a model organic acid having an average p K a of 3.85, an average charge density of 4–5 μeq mg −1 C at ambient pH, and a total of 6–7 meq COOH per gram carbon.

New York↗