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1,722 records · Page 31Linked to original sources
USGS2025

Comparison of creek and bay influences on salt marsh sediment budget and deposition patterns

The resilience of salt marshes with low organic production depends on their effective capture and retention of mineral sediment from adjacent waters. Little prior work has directly compared mechanisms of sediment import from wave-influenced marsh boundaries against those of tidal creeks. We used simultaneous deployment of net-deposition tiles and oceanographic sensors to identify the timing and magnitude of sediment import/export to, and redistribution within, a marsh in south San Francisco Bay. As the marsh has both an eroding bay-exposed scarp and a prominent tidal creek, we investigated the mechanisms and magnitudes of sediment import from the marsh-bay versus the marsh-creek interface. The strong daily sea breezes of the summer season produced most of the wave-driven erosion of the marsh scarp and controlled suspended sediment concentrations; the winter season had weaker winds punctuated by a few storms. A large seasonal difference in suspended sediment concentrations influenced both flood and ebb sediment fluxes to the marsh and led to much higher rates of import in the summer. Both bay-side and creek-side processes were important to total marsh sediment budget. Bay-side sediment contributions were more variable in time due to the bay-influenced environment, and creek-side contributions were overall larger, reflecting the large proportion of the marsh fed by creek water. Sediment was redistributed throughout the system, with erosion near the bay-edge, accretion near the creek-edge and slow import to the marsh interior. The marsh was net importing sediment in the summer and exporting in the winter from different rates of these processes; on an annual scale, the marsh was net importing despite rapid lateral marsh loss. These findings emphasize that a positive sediment budget does not imply a stable marsh and that both creek- and edge-side dynamics are important for marsh sedimentation and geomorphic trajectories. Further, we expand understandings of non-storm and seasonal controls on marsh sedimentation.

California↗
USGS2026

Development of a hydrologic flow model of the Zuñi Salt Lake and surrounding areas, west-central New Mexico

The terminal Zuñi Salt Lake is in a maar in west-​central New Mexico and contains hypersaline water that has long been used by Native Americans for religious purposes and the collection of salt. The U.S. Geological Survey (USGS), in cooperation with the Zuni Tribe of the Zuni Reservation, New Mexico, and Bureau of Reclamation, developed the Zuñi Salt Lake hydrologic flow model to simulate the steady-state conditions of the lake and surrounding groundwater-flow system. The model is a tool that can be used to analyze the potential hydrologic responses to resource development in the region under different water-use scenarios, which can support negotiations that could help protect future use of the lake. The USGS modular hydrologic model, MODFLOW 6, was used to simulate the hydrologic system of the lake and surrounding areas. To define the layering of the model, a three-dimensional hydrogeologic framework was constructed, which included seven informal hydrogeologic units and the locations of faults that truncate and offset the units. Calibration of the model was performed using the iterative ensemble smoother included in a parameter estimation software suite (PEST++). The iterative ensemble smoother approach resulted in a posterior parameter ensemble of model realizations with parameter and simulated values that show similar success in matching observations. Groundwater flux to the Zuñi Salt Lake simulated by using the posterior parameter distribution ranged from 26 to 730 acre-feet per year with a mean, median, and standard deviation of 530, 570, and 170 acre-feet per year, respectively. The relative contribution of groundwater discharge to the lake was simulated using a particle-tracking model for MODFLOW (MODPATH) to be from, in order of decreasing contribution, the Mesaverde, Cenozoic, Mancos, and Dakota hydrogeologic units. Simulations of future conditions using the ensemble of models can provide an empirical estimate of forecast uncertainty without substantial additional analysis.

New Mexico↗
USGS2007

Divisions of geologic time—Major chronostratigraphic and geochronologic units

Effective communication in the geosciences requires consistent uses of stratigraphic nomenclature, especially divisions of geologic time. A geologic time scale is composed of standard stratigraphic divisions based on rock sequences and calibrated in years. Over the years, the development of new dating methods and refinement of previous ones have stimulated revisions to geologic time scales. Since the mid-1990s, geologists from the U.S. Geological Survey (USGS), State geological surveys, academia, and other organizations have sought a consistent time scale to be used in communicating ages of geologic units in the United States. Many international debates have occurred over names and boundaries of units, and various time scales have been used by the geoscience community. For consistency purposes, the USGS Geologic Names Committee and the Association of American State Geologists developed Divisions of Geologic Time .

Fact Sheet↗
USGS2024

3-D mapping of the conterminous U.S. within the USGS National Cooperative Geologic Mapping Program: Progress and future prospects

The U.S. Geological Survey (USGS) National Cooperative Mapping Program (NCGMP) is bringing together subsurface and three-dimensional information at multiple scales for the conterminous United States from data produced throughout the USGS and by federal and state partners. Components of this work include data inventory and catalog development, data integration and database development, and construction of subregional and basin-scale three-dimensional (3-D) geologic models. At small scales, the NCGMP is compiling subsurface data to create a limited number of subsurface layers that map the majority of the lower 48 States. At larger scales, 3-D models of stratigraphic units are intended to be the subsurface analog and extension of the surface geologic maps made within the Program. The Mapping Program is developing methods of storing, visualizing, and distributing 3-D models and subsurface data from multiple sources in easily shareable, queryable, non-proprietary format(s). We report on progress in 3-D mapping of the conterminous U.S. and on future prospects.

conterminous United States↗
USGS2025

Stable isotope composition and geochemistry of calcite and dolomite in the Mountain Pass carbonatite: A lens into petrogenesis

Carbonatites host most of the global rare earth element (REE) deposits. The petrogenesis of these rocks, including magmatic and post-magmatic processes, are poorly understood but critical in forming and upgrading these deposits. The Mountain Pass carbonatite, which hosts the only active REE mine in North America, is lithologically variable but consistently contains >50% calcite and/or dolomite. Multiple generations of carbonates are evident, suggesting bulk analysis of carbonate minerals would generate a mixed isotopic and geochemical signature. In-situ stable carbon and oxygen isotopes, combined with geochemical analysis and petrography, distinguish carbonate generations, trace the source region of the carbonatite magma, and link carbonate genesis to REE mineralization throughout the intrusion. Primary carbon and oxygen isotope values outside the accepted mantle range may suggest a subduction-related carbon and oxygen source in the mantle. Deformation textures in primary calcite indicate syn- or post-crystallization ductile flow. Carbonates with secondary textures and heavy δ 13 C and δ 18 O values are associated with ore mineralization, suggesting fluid mobilization was important in concentrating REE and upgrading of the Mountain Pass deposit.

California↗
USGS2026

Hydrogeologic framework and conceptual groundwater-flow model of the panhandle and northwest parts of the High Plains (Ogallala) aquifer in Oklahoma, 1998–2022

This study was conducted by the U.S. Geological Survey, in cooperation with the Oklahoma Water Resources Board, to update the hydrogeologic framework and conceptual flow model for the panhandle and northwest parts of the High Plains (Ogallala) aquifer in Oklahoma, which together compose the Ogallala aquifer focus area. The study included the construction of a potentiometric surface, and available geologic and hydrologic data were used to evaluate saturated thickness of the aquifer. The water budget for the updated conceptual groundwater-​flow model was based on estimated inflows and outflows for the 1998–2022 study period. Saturated thickness of the Ogallala aquifer averaged 127 and 116 feet for the panhandle and northwest parts, respectively. Groundwater withdrawals from the Ogallala aquifer for 1998–2022 averaged 422,054 and 39,645 acre-feet per year (acre-ft/yr) for the panhandle and northwest parts, respectively. Recharge, the primary inflow, was estimated at 0.63 inch per year for the 1998–2022 study period, with the panhandle part of the Ogallala aquifer receiving 175,068 acre-ft/yr and the northwest part of the Ogallala aquifer receiving 49,376 acre-ft/yr. Additional inflows included irrigation return flows, estimated at 8,111 and 642 acre-ft/yr for the panhandle and northwest parts, respectively, of the Ogallala aquifer. Net lateral groundwater flows, considered to be aquifer outflows, were estimated to account for 31,908 acre-ft/yr for the Ogallala aquifer focus area. Streambed seepage, which was an outflow of 5,535 acre-ft/yr, was only present in the northwest part of the Ogallala aquifer. Vertical leakage and saturated-zone evapotranspiration were considered negligible outflows. These findings provide a revised conceptual groundwater-flow model water budget for the Ogallala aquifer focus area in Oklahoma.

Colorado, Kansas, Oklahoma, Texas↗
USGS2024

Surficial geology and Quaternary fault map of the Las Vegas Valley, Clark County, Nevada

The Surficial Geology and Quaternary Fault Map of the Las Vegas Valley, Clark County, Nevada is a 1:50,000-scale compilation of published 1:24,000-scale geologic maps integrated with new field and desktop mapping. This geologic map compilation and GIS database are part of a broader study on the Quaternary faults in the Las Vegas Valley, the results of which are summarized in this report. The map compilation utilized a variety of digital base maps to evaluate the characteristics of surficial deposits and Quaternary fault scarps including lidar data in undeveloped parts of the valley and orthorectified historical aerial photos in the urbanized center of the valley. The map distinguishes twenty surficial map units including alluvial-fan and ephemeral-wash deposits, groundwater discharge deposits of the Las Vegas Formation, and alluvium deposits of Las Vegas Wash. Quaternary faults include the Quaternary Las Vegas Valley fault system in the center of the valley and the Frenchman Mountain fault system along the eastern margin. All Quaternary fault traces in the valley were evaluated, and the previously published fault mapping was modified as needed. The new mapping and uniform correlation of surficial deposits displaced by Quaternary faults yields a consistent valley-wide characterization of the recency of fault activity. The map and GIS database include a Quaternary geochronology compilation of 119 previously published surficial deposit ages of various types, 35 new luminescence ages, and 3 new radiocarbon ages. The new age data further bracket the ages of the Las Vegas basin Quaternary stratigraphy and provide new constraints on the timing of Quaternary fault activity.

Nevada↗
USGS2025

Examining the role of elevated and sustained strain in dynamically triggering earthquakes on the Anza section of the San Jacinto fault

Microearthquakes can be dynamically triggered in southern California by remote earthquakes. However, directly connecting dynamic triggering mechanisms with observational data remains challenging. One proposed failure mechanism suggests that both the amplitude and duration of cyclic fatigue caused by the passing seismic wave contribute to triggering occurrence. Here, we measure dynamic strains recorded by borehole strainmeters in the Anza section of the San Jacinto fault zone from 710 earthquakes that occurred over 300 km away between 2008 and 2017 to systematically investigate the role of elevated and sustained strain in controlling dynamic triggering. We design a suite of tests to evaluate whether specific amplitude thresholds and durations of strain can predict dynamic triggering cases. We further test whether the peak dynamic strain (PDS) can predict triggering occurrence in combination with the strain amplitude and duration. Based on these tests, there is no strain amplitude–duration threshold that can distinguish triggering occurrence in Anza. Dynamic triggering is more likely to occur if a remote earthquake causes a PDS above 100 nanostrain, though many cases were triggered at smaller PDSs. The lack of clear correlation between triggering and characteristics of the dynamic strain field suggests that the tested features of the incoming waves do not determine triggering occurrence and local fault conditions and slip processes are more important in controlling dynamic triggering in Anza.

California↗
USGS1999

Water quality of Rob Roy Reservoir and Lake Owen, Albany County, and Granite Springs and Crystal Lake Reservoirs, Laramie County, Wyoming, 1997-98

The water quality of four reservoirs was assessed during 1997 and 1998 as a cooperative project between the Cheyenne Board of Public Utilities and the U. S. Geological Survey. The four reservoirs, Rob Roy, Lake Owen, Granite Springs, and Crystal Lake, provide approximately 75 percent of the public water supply for Cheyenne, Wyoming. Samples of water and bottom sediment were collected and analyzed for selected physical, chemical, and biological characteristics to provide data about the reservoirs. Water flows between the reservoirs through a series of pipelines and stream channels. The reservoirs differ in physical characteristics such as elevation, volume, and depth. Profiles of temperature, dissolved oxygen, specific conductance, and pH were examined. Three of the four reservoirs exhibited stratification during the summer. The profiles indicate that stratification develops in all reservoirs except Lake Owen. Stratification developed in Rob Roy, Granite Springs, and Crystal Lake Reservoirs by mid-July in 1998 and continued until September, with the thickness of the epilimnion increasing during that time. Secchi disk readings indicated Rob Roy Reservoir had the clearest water of the four reservoirs studied. The composition of the phytoplankton community was different in the upper two reservoirs from that in the lower two reservoirs. Many of the species found in Rob Roy Reservoir and Lake Owen are associated with oligotrophic, nutrient-poor conditions. In contrast, many of the species found in Granite Springs and Crystal Lake Reservoirs are associated with mesotrophic or eutrophic conditions. The total number of taxa identified also increased downstream. The chemical water type in the reservoirs was similar, but dissolved-solids concentrations were greater in the downstream reservoirs. Water in all four reservoirs was a calcium-bicarbonate type. In the fall of 1997, Rob Roy Reservoir had the lowest dissolved-solids concentration (19 milligrams per liter), whereas Crystal Lake Reservoir had the highest concentration (63 milligrams per liter). Relatively little differences in the concentrations of major-ion species were noted between samples collected near the surface and near the bottom of the same reservoir. In contrast, iron and manganese concentrations generally were higher in samples collected near the bottom of a reservoir than in near-surface samples collected from the same reservoir. Composite bottom-sediment samples from all four reservoirs contained similar concentrations of bulk constituents such as aluminum, iron, phosphorus and titanium, but varied in concentrations of trace elements. Trace-element concentrations in Rob Roy Reservoir and Lake Owen were similar to the crustal average, whereas in Granite Springs and Crystal Lake Reservoirs the concentrations were similar to granitic rocks.

Wyoming↗
USGS2023

Surficial geologic map of the Owlshead Mountains 30' x 60' quadrangle, Inyo and San Bernardino Counties, California

The surficial geologic map of the Owlshead Mountains 30' x 60' quadrangle depicts the distribution and characteristics of surficial-deposit materials and neotectonic deformation for an area of approximately 5,000 square kilometers (km 2 ) located in the western Basin and Range Province of eastern California. The map represents a new compilation of the surficial geology that encompasses deposits within the late Pliocene to Quaternary. The map is based primarily on new mapping conducted between 2001 and 2009. Map compilation was supported by field observations distributed across the map area, combined with reference to several published and unpublished mapping sources that mostly emphasized neotectonic deformation. The surficial-deposit units included in the map follow a classification scheme that systematically denotes depositional process, relative age, and any secondary sedimentologic or morphologic characteristics. Identification, correlation, and age estimation of map units are based primarily on the relative degree of development of certain time-dependent characteristics such as surface morphology, including local dissection and surface preservation, surface clast modification, and degree of soil development; these characteristics are implicitly incorporated into unit designations. The map represents a detailed and regionally uniform synthesis of the late Neogene geology for this large area that provides a framework applicable to many interpretative studies, such as regional patterns of deposition and dissection; surface drainage development and evolution; and the distribution, style, and timing of neotectonic deformation.

California↗
USGS2024

Characterization of groundwater resources near the southeastern part of Puget Sound, Washington

More than 1 million people live within the active model area (AMA) in the southeastern part of the lowlands surrounding Puget Sound, or Puget Lowland, Washington, and groundwater is the source for approximately one-half of their public, domestic, and irrigation water demands. The 887-square-mile AMA, located in King and Pierce Counties, represents the area of analysis for the conceptual hydrogeologic framework and numerical groundwater-flow models within the study area and includes the Puyallup River and Chambers-Clover Creek watersheds. To assess the potential hydrologic and anthropogenic impacts to groundwater and the connected surface-water resources, conceptual and numerical groundwater-flow models of groundwater flow were developed by the U.S. Geological Survey Washington Water Science Center in close cooperation with 18 water-resource agencies and stakeholders. This multichapter volume documents the development of the conceptual and numerical groundwater-flow models of groundwater flow. Chapters A, B, and C provide an overall introduction to the multichapter volume (Chapter A), the conceptual hydrogeologic framework (Chapter B), and the groundwater budget (Chapter C). Chapters D and E describe numerical groundwater-flow model construction and calibration (Chapter D) and the numerical groundwater-flow model results (Chapter E). Collectively, these reports present a characterization and simulation tool for groundwater resources near the southeastern part of Puget Sound, Washington.

Scientific Investigations Report↗
USGS2025

Summary of selenium in the lower Gunnison River Basin, Colorado—Information and data gaps

The Cretaceous Mancos Shale is a geologic source of selenium in the lower Gunnison River Basin. Natural weathering processes and human activity mobilize selenium from the Mancos Shale and derived materials, and surface water, groundwater, and sediment all affect the transport of selenium from source areas to receiving streams and biota. Selenium accumulates through the aquatic food chain, and its toxic effects can result in invertebrate mortality and mortality, decreased reproduction, and deformities to fish and birds. The Bureau of Reclamation, in cooperation with the State of Colorado and Gunnison River Basin water users, is implementing a Selenium Management Program to reduce selenium concentrations in the lower Gunnison River Basin of Colorado. Goals of the Selenium Management Program are to (1) achieve compliance with the State of Colorado chronic aquatic-life standard for dissolved selenium (4.6 micrograms per liter) in the Gunnison River near Grand Junction, Colorado; (2) sufficiently improve water-quality conditions to assist in the recovery of endangered species in the Gunnison and Colorado Rivers by reducing selenium concentrations; and (3) support continued water uses in the basin. Many previous studies have contributed to the understanding of selenium in the environment; however, monitoring and research data gaps exist in the lower Gunnison River Basin. The purpose of this report is to summarize information regarding selenium in the lower Gunnison River Basin and describe strategies for scientific research and monitoring to potentially improve understanding of selenium sources; processes affecting the mobilization, transport, and fate of selenium; and the effects of selenium-mitigation projects in the lower Gunnison River Basin. Monitoring and research data gaps discussed in this report include geologic mapping and geochemical source characterization, long-term and ongoing monitoring of the surface-water and groundwater networks, developing and refining statistical models, characterizing selenium on suspended sediment, modeling selenium in the food web, evaluating best management practices, and more.

Colorado↗
USGS2024

Geophysical characterization of mine influenced groundwater and surface water in the Mayflower section of the Animas River, Bonita Peak Mining District, Silverton Colorado

This report details findings from geophysical investigations to identify possible groundwater - surface water interactions near the Mayflower Section of the Animas River in Silverton, Colorado. The Mayflower Section is a mine influenced Superfund Site in Colorado. This investigation utilized electromagnetic induction (EM or EMI), magnetic, and fiber optic distributed temperature system (FODTS) geophysical methods to measure the bulk earth electrical conductivity, magnetic susceptibility, and temperature of specific surveyed volumes of the earth near the Mayflower Section of the Animas River. These physical parameters are used to understand the groundwater – surface water interactions, which can guide decision makers in their assessment of mine-impacted surface water. This report details the results from characterization and monitoring technologies to provide high data density and continuous monitoring of bulk earth electrical conductivity and temperature in the Mayflower section of the Animas River to identify zones of groundwater – surface water interactions and potential metal loading from mine influenced water. The investigation separated right and left bank characterization for each method and indicates more groundwater is entering from the right bank than the left bank and these predominantly right bank discharges potentially contain metal-rich water compared to the left bank. Results also indicate mineral veins facilitate preferential groundwater discharge to the river due to possible jointing, fractures, and permeability differences sometimes occurring along veins relative to host rock. For example, Boulder Gulch is likely groundwater dominated and may be receive water impacted by Mayflower Impoundments #1 and #2. Additionally, the beaver ponds near Blair Gulch may influence groundwater discharge and Mayflower Impoundment #4 is possibly impacting groundwater and surface water and may be connected to the wetlands to the west of the impoundment. These data could be further analyzed for smaller spatial scale analysis within areas of interest. The identification of these locations along sections of the river likely impacted by mine influenced groundwater potentially entering the Animas River and can be used by site investigators, decision makers, and stakeholders in mitigation decisions and strategies.

Colorado↗
USGS2025

Comparison of hydrologic data and water budgets between 2003–08 and 2018–23 for the eastern part of the Arbuckle-Simpson aquifer, south-central Oklahoma

The Arbuckle-Simpson aquifer is divided spatially into three parts (eastern, central, and western). The largest groundwater withdrawals are from the eastern part of the Arbuckle-Simpson aquifer, which provides water to approximately 39,000 people in Ada and Sulphur, Oklahoma, and surrounding areas. The Arbuckle-Simpson aquifer, including the eastern part, is designated a sole source aquifer for its service area. Based primarily on data collected between 2003 and 2008, a series of comprehensive hydrologic studies of the Arbuckle-Simpson aquifer was published to provide the information necessary to perform groundwater-flow model simulations so that the Oklahoma Water Resources Board could determine how much water could be withdrawn from the aquifer while maintaining flow to springs and streams. As part of the Phase 1 studies, an aquifer water budget was developed from a numerical model for the period 2003–08. For this report, Phase 1 refers to the 2003–08 data collection period, although for some of the analyses, data collected prior to 2003 were used to inform model development work. Allocation of water from this aquifer was then established by the Oklahoma Water Resources Board in 2013. Additional well-spacing rules were also established by the Oklahoma Water Resources Board for sensitive sole source groundwater basins. To determine how the water budget for the eastern part of the Arbuckle-Simpson aquifer has changed over time, recently collected hydrologic data (2018–23) were compared to data collected during 2003–08. The analysis of changes in the aquifer water budget from 2003–08 to 2018–23 could help resource managers better understand changes in the overall balance of water in storage and the potential effects on streamflow, changes in groundwater levels, and the effects of different water uses in the aquifer area on available water in the eastern part of the Arbuckle-Simpson aquifer and streams overlying the eastern part of the Arbuckle-Simpson aquifer.

Oklahoma↗
USGS2026

End-user needs for remote sensing wetlands of the Prairie Pothole Region of North America

The Prairie Pothole Region (PPR) of North America comprises globally important grassland and wetland ecosystems critical for numerous populations of migratory birds. Due to the importance of this region for migratory birds, and particularly waterfowl, and the threats of habitat loss due to intensifying agriculture, there is a mature and diverse system of conservation organizations, agencies, and partnerships that spends hundreds of millions of dollars annually on habitat conservation to support migratory bird populations. Remote sensing can be a powerful tool for observing and evaluating global change at large scales as well as expanding inferences from field studies to the broader landscape with statistical models. However, development and utilization of these tools has lagged behind their demand for several reasons, including concerns over spatial and temporal resolution and accuracy of products; perception of a misalignment with decision-maker needs; technological barriers such as skill sets of conservation professionals, computing resources, data access, and usability. In this report, we summarize the needs of conservation professionals and scientists who use or want to use remote sensing data products to inform science about wetland change and conservation of wetlands in the PPR. We assembled this information through several methods leading up to, during, and following a January 2026 PPR Wetland Remote Sensing Workshop. The workshop included United States and Canadian scientists, conservation professionals, and policy experts. Our goal was to bring together end-users and remote sensing product developers jointly to explore reducing the lag between product development and utilization of products to inform science and conservation. Specifically, we aimed to identify gaps in wetland remote sensing that limit effective monitoring, management, and conservation in the PPR, and to develop a framework that outlines pathways to address these gaps by fostering collaboration, improving communication networks, encouraging discussion, and building on existing and ongoing efforts. This report summarizes our participants’ descriptions of end-user needs and the outcomes of the workshop.

Prairie Pothole region↗
USGS2025

Determination of per- and polyfluoroalkyl substances in water by direct injection of matrix-modified centrifuge supernatant and liquid chromatography/tandem mass spectrometry with isotope dilution

A direct-injection liquid chromatography/tandem mass spectrometry method was developed to determine 34 per- and polyfluoroalkyl substances (PFAS), including selected branched isomers, in centrifuge supernatant of matrix-modified (amended with approximately 50 percent methanol) water samples. The method has been validated in reagent water, surface water, groundwater, and wastewater effluent. Other water types (for example, drinking water, untreated wastewater, and landfill leachate) have been analyzed by the method but not systematically validated. Recovery of isotope-dilution standards, added to each sample, may be used to assess method performance in nonvalidated matrices on a sample-by-sample basis. Using this method, PFAS concentrations were determined in the range of 2–2,000 nanograms per liter in water samples. This range can be extended by diluting concentrated samples. At circumneutral pH, most compounds are present in the environment in their ionized form, and data are reported as such (for example, perfluorooctanoic acid is referred to as “perfluorooctanoate” [PFOA], perfluorooctane sulfonic acid is referred to as “perfluorooctane sulfonate” [PFOS]). Sample preparation procedures were designed without the use of filtration and with minimum sample handling steps to mitigate procedural losses of target compounds due to sorption to surfaces. Further, isotope-dilution quantification allowed for the correction of bias that may result from procedural losses, matrix-induced signal suppression or enhancement, and other factors. Validation experiments to characterize bias and variability, method detection level, and holding time were done in four distinct water matrices—reagent water, surface water, treated wastewater effluent, and groundwater—at multiple concentration levels. Mean PFAS recoveries met data quality objectives of bias and variability studies in all four validation matrices except for two compounds with low and variable recovery in the reagent water matrix only. Isotope-dilution standards, treated as surrogate compounds, were analyzed in more than 1,500 customer-submitted environmental samples with aggregate recovery of 102.5±6.5 percent (mean±standard deviation). Maximum holding times for all target compounds in the four validation matrices were 28 days for refrigerated samples and 90 days for frozen samples.

Techniques and Methods↗