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Determination of the δ 34 S of low-concentration sulfate in water; RSIL lab code 1949

The purpose of the Reston Stable Isotope Laboratory (RSIL) lab code 1949 is to determine the δ( 34 S/ 32 S), abbreviated as δ 34 S, of dissolved sulfate having a concentration less than 20 milligrams per liter. Dissolved sulfate is collected on an anion-exchange resin in the field, eluted in the laboratory with 3 M KCl, and precipitated with BaCl 2 at pH 3 to 4 as BaSO 4 . The precipitated BaSO 4 is filtered and dried before introduction into an elemental analyzer (EA) Carlo Erba NC 2500. The EA is used to convert sulfur in a BaSO 4 solid sample into SO 2 gas, and the EA is connected to a continuous flow isotope-ratio mass spectrometer (CF-IRMS), which determines differences in the isotope-amount ratios of stable sulfur isotopes ( 34 S/ 32 S) of the product SO 2 gas. The combustion is quantitative; no isotopic fractionation is involved. Samples are placed in a tin capsule and loaded into the Costech Zero Blank Autosampler of the EA. Under computer control, samples are dropped into a heated reaction tube that combines the oxidation and reduction reactions. The combustion takes place in a helium atmosphere containing an excess of oxygen gas at the oxidation zone at the top of the reaction tube. Combustion products are transported by a helium carrier through the reduction zone at the bottom of the reaction tube to remove excess oxygen and through a separate drying tube to remove any water. The gas-phase products, mainly CO 2 , N 2 , and SO 2 , are separated by a gas chromatograph. The gas is then introduced into the isotope-ratio mass spectrometer (IRMS) through a Finnigan MAT (now Thermo Scientific) ConFlo II interface, which is also used to inject SO 2 reference gas and helium for sample dilution. The IRMS is a Thermo Scientific Delta V Plus CF-IRMS. It has a universal triple collector with two wide cups and a narrow cup in the middle. It is capable of measuring mass/charge ( m/z ) 64 and 66 simultaneously. The ion beams from SO 2 are as follows: m/z 64 = SO 2 = 32 S 16 O 16 O; m/z 66 = SO 2 = 34 S 16 O 16 O primarily.

Techniques and Methods↗

FGDC Digital Cartographic Standard for Geologic Map Symbolization (PostScript Implementation)

PLEASE NOTE: This now-approved 'FGDC Digital Cartographic Standard for Geologic Map Symbolization (PostScript Implementation)' officially supercedes its earlier (2000) Public Review Draft version (see 'Earlier Versions of the Standard' below). In August 2006, the Digital Cartographic Standard for Geologic Map Symbolization was officially endorsed by the Federal Geographic Data Committee (FGDC) as the national standard for the digital cartographic representation of geologic map features (FGDC Document Number FGDC-STD-013-2006). Presented herein is the PostScript Implementation of the standard, which will enable users to directly apply the symbols in the standard to geologic maps and illustrations prepared in desktop illustration and (or) publishing software. The FGDC Digital Cartographic Standard for Geologic Map Symbolization contains descriptions, examples, cartographic specifications, and notes on usage for a wide variety of symbols that may be used on typical, general-purpose geologic maps and related products such as cross sections. The standard also can be used for different kinds of special-purpose or derivative map products and databases that may be focused on a specific geoscience topic (for example, slope stability) or class of features (for example, a fault map). The standard is scale-independent, meaning that the symbols are appropriate for use with geologic mapping compiled or published at any scale. It will be useful to anyone who either produces or uses geologic map information, whether in analog or digital form. Please be aware that this standard is not intended to be used inflexibly or in a manner that will limit one's ability to communicate the observations and interpretations gained from geologic mapping. In certain situations, a symbol or its usage might need to be modified in order to better represent a particular feature on a geologic map or cross section. This standard allows the use of any symbol that doesn't conflict with others in the standard, provided that it is clearly explained on the map and in the database. In addition, modifying the size, color, and (or) lineweight of an existing symbol to suit the needs of a particular map or output device also is permitted, provided that the modified symbol's appearance is not too similar to another symbol on the map. Be aware, however, that reducing lineweights below .125 mm (.005 inch) may cause symbols to plot incorrectly if output at higher resolutions (1800 dpi or higher). For guidelines on symbol usage, as well as on color design and map labeling, please refer to the standard's introductory text. Also found there are informational sections covering concepts of geologic mapping and some definitions of geologic map features, as well as sections on the newly defined concepts and terminology for the scientific confidence and locational accuracy of geologic map features. More information on both the past development and the future maintenance of the FGDC Digital Cartographic Standard for Geologic Map Symbolization can be found at the FGDC Geologic Data Subcommittee website (http://ngmdb.usgs.gov/fgdc_gds/). Earlier Versions of the Standard

Techniques and Methods↗

Federal standards and procedures for the National Watershed Boundary Dataset (WBD)

The Watershed Boundary Dataset (WBD) is a seamless, national hydrologic unit dataset developed using the guidelines and specifications outlined in this document. A hydrologic unit defines the areal extent of surface-water drainage to an outlet point on a dendritic stream network or to outlet points where the stream network is not dendritic. A hydrologic unit may represent all or only part of the total drainage area to the outlet point so that multiple hydrologic units may be required to define the entire drainage area for a given outlet. Hydrologic unit boundaries in the WBD are determined on the basis of topographic, hydrologic, and other relevant landscape characteristics without regard for administrative, political, or jurisdictional boundaries. The WBD seamlessly represents hydrologic units at six required and two optional hierarchical levels mapped at a minimum of 1:24,000-scale in the United States, except for in Hawaii, the Caribbean, and the Pacific Islands, which are at 1:25,000-scale, and in Alaska, where the data range from the minimum required 1:24,000-scale to 1:63,360-scale. Hydrologic units in the WBD provide a standardized base for water-resources organizations to locate, store, retrieve, and exchange hydrologic data; to index and inventory hydrologic data and information; to catalog water-data acquisition activities; and to use in a variety of other applications. The specifications and procedures established in this document are intended to provide guidelines and best practices to local, regional, and national partners for delineating and updating the hydrologic units of the WBD. Maintaining the WBD using consistent practices improves watershed management through efficient sharing of information and resources and by ensuring that digital geographic data can be used with other related geographic information system data. Edits and additions to the hydrologic units are reviewed against this specification prior to inclusion to the national WBD.

Techniques and Methods↗

Standard for the U.S. Geological Survey Historical Topographic Map Collection

This document defines the digital map product of the U.S. Geological Survey (USGS) Historical Topographic Map Collection (HTMC). The HTMC is a digital archive of about 190,000 printed topographic quadrangle maps published by the USGS from the inception of the topographic mapping program in 1884 until the last paper topographic map using lithographic printing technology was published in 2006. The HTMC provides a comprehensive digital repository of all scales and all editions of USGS printed topographic maps that is easily discovered, browsed, and downloaded by the public at no cost. Each printed topographic map is scanned “as is” and captures the content and condition of each map. The HTMC provides ready access to maps that are no longer available for distribution in print. A new generation of topographic maps called “US Topo” was defined in 2009. US Topo maps, though modeled on the legacy 7.5-minute topographic maps, conform to different standards. For more information on the HTMC, see the project Web site at: http://nationalmap.gov/historical/ .

Techniques and Methods↗

Selection of colors and patterns for geologic maps of the U.S. Geological Survey

U.S. Geological Survey (USGS) color and pattern standards and conventions for geologic maps have evolved since the USGS published its first set of standards in 1881. Since that time, USGS personnel have continuously updated and revised the standards in response to the need to show increasingly complex geologic map data and in response to changing technology. The color and pattern standards and conventions contained in this book enable geologists, cartographers, and editors to produce geologic maps that have consistent geologic-age color schemes and patterns. Such consistency enables geologists and other users of geologic maps to obtain a wealth of geologic information at a glance and to produce maps that can easily be used and compared to other published maps that follow the color and pattern standards and conventions.

Techniques and Methods↗

GeMS (Geologic Map Schema)—A standard format for the digital publication of geologic maps

Introduction This report describes and defines GeMS (for Ge ologic M ap S chema), a new standardized database schema—that is, a database design—for the digital publication of geologic maps. It originally was intended for geologic mapping funded by the National Cooperative Geologic Mapping Program of the U.S. Geological Survey, but its use can be extended to other programs and agencies as well. It is intended to bridge the gap between traditional geologic mapping and GIS communities at an operational level. GeMS provides for the encoding in digital form of the content contained in individual geologic maps published by the U.S. Geological Survey and by state geological surveys. The design is focused on the publication, transfer, and archiving of map data and less on the creation of map data, the visual representation of map data, or the compilation of data from many different map sources. Although GeMS is designed for a single-map database, it also is intended to provide a stepping stone toward the development of multiple-map databases, in particular the National Geologic Map Database. The database design contained herein will significantly promote that goal. All questions or comments about GeMS should be directed via email to gems@usgs.gov .

Techniques and Methods↗

Elevation-derived hydrography—Representation, extraction, attribution, and delineation rules

With the increasing availability of 3D Elevation Program (3DEP) quality high resolution elevation data across the United States and the pressing need for better integrated elevation and hydrography data, the U.S. Geological Survey is developing guidance to improve the horizontal and vertical alignment of these datasets. The U.S. Geological Survey is providing the Elevation-Derived Hydrography—Acquisition Specifications for the acquisition of elevation-derived hydrography for the United States, and the companion document The Elevation-Derived Hydrography—Representation, Extraction, Attribution, and Delineation (READ) Rules, which describes the parameters for the portrayal of hydrography features as derived from elevation data. The READ Rules provide a definition, example, attribute value list, delineation instructions, representation rules, and data extraction rules for each hydrography feature required to meet the Elevation-Derived Hydrography—Acquisition Specifications.

Techniques and Methods↗

Planetary geologic mapping protocol—2022

The Planetary Geologic Mapping Protocol covers the idealized process of compiling a NASA-funded map product of a non-terrestrial solid surface planetary body for U.S. Geological Survey (USGS) publication and summarizes technical specifications of the Mapping Process for authors and reviewers. Directed by community and programmatic recommendations, the USGS Planetary Geologic Map Coordination Group assembled the content herein to aid the timely production of USGS map products. This document can be also used as a reference document by those researchers who are completing geologic maps that will be published outside the USGS.

Techniques and Methods↗

User’s Guide to planetary image analysis and geologic mapping in ArcGIS Pro

Geologic maps are valuable tools in planetary science. Though planetary geologic maps are similar to terrestrial (Earthbased) geologic maps, the nature of planetary exploration introduces unique challenges for geologic mappers. Terrestrial geologic mappers prepare products from field-based observation, often comparing or refining those with aerial and (or) orbital images. Planetary geologic mapping relies almost exclusively on remote observations, which are made by orbiting spacecraft. Therefore, with a few exceptions for locations with rovers, landers, or crewed surface missions, planetary geologic mappers are not able to observe their map area in detail or at smaller scales. As a result, they must interpret and describe their map features differently than those used in terrestrial geologic maps. For example, terrestrial geologic mappers commonly divide units by lithology (rock type) or grain size. However, planetary geologic mappers often do not have detailed enough information to know what type of rock or grain size is present, and instead must divide the planet’s surface into geologic units using differences in tone, color, and surface texture (at multiple scales). Cross-cutting relationships, where apparent, can provide excellent—and often crucial—observations for identifying and subdividing geologic units using orbital datasets. The process of creating planetary maps has evolved over time, from original hand-drawn maps created during the early 1800s through the late 1900s, to the fully digital products created today. Modern-day planetary geologic mapping uses Geographic Information Systems (GIS) software and tools to visualize data, delineate units and landforms, and accurately convey spatial relationships to a map user using cartographic features represented by points, lines, and polygons. This tutorial was written to familiarize both new and experienced planetary geologic mappers with ArcGIS Pro, a commonly used GIS software package developed by Esri. This tutorial introduces new planetary geologic mappers to fundamental concepts and best practices in planetary geologic mapping. For mappers with experience using ArcMap (a previous version of ArcGIS), this tutorial will help to familiarize users with new changes in layout and functionality, so current projects may be migrated into the ArcGIS Pro environment. No prior knowledge is required, although a general familiarity with geology, GIS, and planetary science is recommended. This tutorial includes links to helpful glossaries of common GIS terms and other GIS and planetary science resources in appendix 1. For additional information on planetary geologic mapping, see the U.S Geological Survey (USGS) Astrogeology NASA Planetary Geologic Mapping Program website and the Planetary Mapping Guidelines. Numerous ArcGIS tutorials are also available from Esri’s Tutorials page, through the Esri Academy catalog, and Esri’s ArcGIS Pro Resources page.

Techniques and Methods↗

US Topo Product Standard

This document defines a U.S. Geological Survey (USGS) digital topographic map. This map product series, named “US Topo,” is modeled on the now historical USGS 7.5-minute (1:24,000 scale) topographic map series produced and printed by the USGS from 1947 to 2006. US Topo maps have the same extent, scale, and general layout as the historical topographic maps. US Topo maps incorporate an orthorectified image (hereinafter referred to as “orthoimage”) and shaded relief image along with a selection of data that were included in the historical 7.5-minute topographic maps. Between June and September of 2017, the USGS transitioned the format of US Topo maps to be published, by using a geospatial extension, in an International Organization for Standardization (ISO) 32000-compliant Adobe® portable document format (PDF) that is called a “geospatial PDF.” Previously, US Topo maps were published, by using geospatial extensions patented by TerraGo® Technologies, in PDF in a format called a “GeoPDF®.” The geospatial PDF design allows a user to zoom in and out in a georeferenced environment, turn layers on and off, view or print any combination of layers, and print any portion of the map at the published scale. US Topo maps are intended to serve conventional map users by providing geographic information system (GIS) information in symbolized form in the customary topographic map layout. The maps are not intended for advanced GIS analysis applications. These products are built on standard coordinate systems and include full U.S. National Grid (USNG) lines, making US Topo maps particularly useful for emergency first-response operations. These maps are also used by traditional topographic map users, such as resource managers, planners, and recreational users who continue to have a need for the symbolized feature data contained in the 7.5-minute quadrangle maps. Full-size style sheet templates in PDF defining the placement of map elements, marginalia, and font sizes and styles accompany this standard. US Topo maps published as geospatial PDFs are fashioned to conform to these style sheets so that a user can print out a map at the 1:24,000, 1:25,000, or 1:20,000 scale using the dimensions of the traditional standard 7.5-minute quadrangle. Symbology and type specifications for feature content and detailed requirements for geospatial content will be published separately. This document is an update of the US Topo Product Standard published in 2011 (Cooley and others, 2011). It is applicable to all US Topo maps. Updates in this version include the introduction of an ISO 32000-compliant geospatial PDF as a new file format for published maps; new style sheet templates for 1:24,000-scale maps (conterminous United States and Hawaii), 1:25,000-scale maps (Alaska), and 1:20,000-scale maps (Puerto Rico and U.S. Virgin Islands); an updated US Topo Map Symbol attachment; minor updates to text, including changes to the features and layers included in the US Topo product and the sheet size of the US Topo maps; updated figures demonstrating the US Topo product; an updated metadata file containing map-specific information.

Techniques and Methods↗

Lidar base specification

In late 2009, a $14.3 million allocation from the American Recovery and Reinvestment Act (ARRA) for new light detection and ranging (lidar) elevation data acquisition prompted the U.S. Geological Survey (USGS) National Geospatial Program (NGP) to develop a common minimum specification for all lidar data acquired for The National Map. Released as a working draft in 2010 and formally published in 2012, the USGS–NGP Lidar Base Specification (LBS) was quickly embraced by numerous States, counties, and foreign countries as the foundation for their own lidar specifications. Prompted by a growing appreciation for the wide applicability and inherent value of lidar, a consortium of Federal agencies commissioned the National Enhanced Elevation Assessment (NEEA) study in 2010 to quantify the costs and benefits of a national lidar program. Published in 2012, the NEEA report documented a substantial return on such an investment, defined five quality levels (QL) for elevation data, and recommended an 8-year collection cycle of QL2 lidar data as the optimum balance of benefit and affordability. In response to the study, the USGS–NGP established the 3D Elevation Program (3DEP) in 2013 as the interagency vehicle through which the NEEA recommendations could be realized. Lidar is a quickly evolving technology and much has changed in the industry since the previous version of the Lidar Base Specification (LBS) was published. Lidar data have improved in accuracy and spatial resolution, the American Society for Photogrammetry and Remote Sensing has revised the geospatial accuracy standards, industry standard file formats have been expanded, additional applications for lidar have become accepted, and the need for interoperable data across collections has been realized. This revision to the LBS addresses some of those changes and provides continued guidance towards a nationally consistent lidar dataset. Note Future versions of the Lidar base specification will be released online at https://www.usgs.gov/3DEP/lidarspec .

Techniques and Methods↗

Digital orthoimagery base specification V1.0

The resolution requirement for orthoimagery in support of the The National Map of the U.S. Geological Survey (USGS) is 1 meter. However, as the Office of Management and Budget A-16 designated Federal agency responsible for base orthoimagery, the USGS National Geospatial Program (NGP) has developed this base specification to include higher resolution orthoimagery. Many Federal, State, and local programs use high-resolution orthoimagery for various purposes including critical infrastructure management, vector data updates, land-use analysis, natural resource inventory, and extraction of data. The complex nature of large-area orthoimagery datasets, combined with the broad interest in orthoimagery, which is of consistent quality and spatial accuracy, requires high-resolution orthoimagery to meet or exceed the format and content outlined in this specification. The USGS intends to use this specification primarily to create consistency across all NGP funded and managed orthoimagery collections, in particular, collections in support of the National Digital Orthoimagery Program (NDOP). In the absence of other comprehensive specifications or standards, the USGS intends that this specification will, to the highest degree practical, be adopted by other USGS programs and mission areas, and by other Federal agencies. This base specification, defining minimum parameters for orthoimagery data collection. Local conditions in any given project area, specialized applications for the data, or the preferences of cooperators, may mandate more stringent requirements. The USGS fully supports the acquisition of more detailed, accurate, or value-added data that exceed the base specification outlined herein. A partial list of common “buy-up” options is provided in appendix 1 for those areas and projects that require more stringent or expanded specifications.

Techniques and Methods↗

Specification for the U.S. Geological Survey Historical Topographic Map Collection

This document provides the detailed requirements for producing, archiving, and disseminating a comprehensive digital collection of topographic maps for the U.S. Geological Survey (USGS) Historical Topographic Map Collection (HTMC). The HTMC is a digital archive of about 190,000 printed topographic maps published by the USGS from the inception of the topographic mapping program in 1884 until the last paper topographic map using lithographic printing technology was published in 2006. The HTMC provides a comprehensive digital repository of all scales and all editions of USGS printed topographic maps that is easily discovered, browsed, and downloaded by the public at no cost. The HTMC provides ready access to maps that are no longer available for distribution in print. A digital file representing the original paper historical topographic map is produced for each historical map in the HTMC in georeferenced PDF (GeoPDF) format (a portable document format [PDF] with a geospatial extension).

Techniques and Methods↗

1-Meter Digital Elevation Model specification

In January 2015, the U.S. Geological Survey National Geospatial Technical Operations Center began producing the 1-Meter Digital Elevation Model data product. This new product was developed to provide high resolution bare-earth digital elevation models from light detection and ranging (lidar) elevation data and other elevation data collected over the conterminous United States (lower 48 States), Hawaii, and potentially Alaska and the U.S. territories. The 1-Meter Digital Elevation Model consists of hydroflattened, topographic bare-earth raster digital elevation models, with a 1-meter x 1-meter cell size, and is available in 10,000-meter x 10,000-meter square blocks with a 6-meter overlap. This report details the specifications required for the production of the 1-Meter Digital Elevation Model.

Techniques and Methods↗

The National Map seamless digital elevation model specifications

This specification documents the requirements and standards used to produce the seamless elevation layers for The National Map of the United States. Seamless elevation data are available for the conterminous United States, Hawaii, Alaska, and the U.S. territories, in three different resolutions—1/3-arc-second, 1-arc-second, and 2-arc-second. These specifications include requirements and standards information about source data requirements, spatial reference system, distribution tiling schemes, horizontal resolution, vertical accuracy, digital elevation model surface treatment, georeferencing, data source and tile dates, distribution and supporting file formats, void areas, metadata, spatial metadata, and quality assurance and control.

Techniques and Methods↗

Analyzing legacy U.S. Geological Survey geochemical databases using GIS: applications for a national mineral resource assessment

This report emphasizes geographic information system analysis and the display of data stored in the legacy U.S. Geological Survey National Geochemical Database for use in mineral resource investigations. Geochemical analyses of soils, stream sediments, and rocks that are archived in the National Geochemical Database provide an extensive data source for investigating geochemical anomalies. A study area in the Egan Range of east-central Nevada was used to develop a geographic information system analysis methodology for two different geochemical datasets involving detailed (Bureau of Land Management Wilderness) and reconnaissance-scale (National Uranium Resource Evaluation) investigations. ArcGIS was used to analyze and thematically map geochemical information at point locations. Watershed-boundary datasets served as a geographic reference to relate potentially anomalous sample sites with hydrologic unit codes at varying scales. The National Hydrography Dataset was analyzed with Hydrography Event Management and ArcGIS Utility Network Analyst tools to delineate potential sediment-sample provenance along a stream network. These tools can be used to track potential upstream-sediment-contributing areas to a sample site. This methodology identifies geochemically anomalous sample sites, watersheds, and streams that could help focus mineral resource investigations in the field.

Egan Range↗

User’s manual to update the National Wildlife Refuge System Water Quality Information System (WQIS)

National Wildlife Refuges may have impaired water quality resulting from historic and current land uses, upstream sources, and aerial pollutant deposition. National Wildlife Refuge staff have limited time available to identify and evaluate potential water quality issues. As a result, water quality–related issues may not be resolved until a problem has already arisen. The National Wildlife Refuge System Water Quality Information System (WQIS) is a relational database developed for use by U.S. Fish and Wildlife Service staff to identify existing water quality issues on refuges in the United States. The WQIS database relies on a geospatial overlay analysis of data layers for ownership, streams and water quality. The WQIS provides summary statistics of 303(d) impaired waters and total maximum daily loads for the National Wildlife Refuge System at the national, regional, and refuge level. The WQIS allows U.S. Fish and Wildlife Service staff to be proactive in addressing water quality issues by identifying and understanding the current extent and nature of 303(d) impaired waters and subsequent total maximum daily loads. Water quality data are updated bi-annually, making it necessary to refresh the WQIS to maintain up-to-date information. This manual outlines the steps necessary to update the data and reports in the WQIS.

Techniques and Methods↗