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Identification of thermal maturity-relevant organic matter in Shale Working Group Report 2021

Abstract

The Identification of Thermal Maturity-Relevant Organic Matter in Shale Working Group of the ICCP was established in 2008 to provide guidelines for identifying and measuring the reflectance of the population of dispersed organic matter that is relevant to thermal maturity determination. Information products published by the working group include ASTM D7708 Standard Test Method for Microscopical Determination of the Reflectance of Vitrinite Dispersed in Sedimentary Rocks (ASTM, 2014) and two interlaboratory studies (ILS) to determine precision statistics for this ASTM test method (Hackley et al., 2015, 2020). Poor reproducibility of solid bitumen and vitrinite reflectance measurements in the second ILS (Hackley et al., 2020) suggested that further work is required to standardize the identification of thermal maturity-relevant dispersed organic matter for reproducible reflectance measurements. Thus, at the 2019 ICCP meeting in The Hague, Netherlands, the working group decided to pursue additional ILS via image-based approaches to improve reproducibility.

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BibTeXRIS

Paul C. Hackley, Javin J. Hatcherian, Jennifer L. Rivera, Margaret M. Sanders, Brett J. Valentine. 2022. Identification of thermal maturity-relevant organic matter in Shale Working Group Report 2021. https://pubs.usgs.gov/publication/70230399

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Finalization of the Confocal Laser Scanning Microscopy (CLSM) working group

A working group in Commission II to investigate applications of confocal laser scanning microscopy (CLSM) for organic petrology investigations has finalized with publication of the manuscript “Characterization of bituminite in Kimmeridge Clay by confocal laser scanning and atomic force microscopy” in the International Journal of Coal Geology. The manuscript is available via Open Access from https://doi.org/10.1016/j.coal.2022.103927 and also from the Commission II working group (WG) webpage https://www.iccop.org/workinggroup/confocal-laser-scanning-microscopy-clsm/. A report detailing the full history and results from the WG also is available from the Commission II WG webpage. The working group investigated the application of CLSM to an organic-rich (44 wt.% TOC), thermally immature sample (VRo 0.42%) of the Kimmeridge Clay Formation. CLSM imaging and spectroscopy and atomic force microscopy (AFM) were used to characterize bituminite.

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